International
Tables for
Crystallography
Volume C
Mathematical, physical and chemical tables
Edited by E. Prince

International Tables for Crystallography (2006). Vol. C, ch. 10.2, pp. 962-963

Section 10.2.2. Sealed sources and radiation-producing apparatus

D. C. Creagha and S. Martinez-Carrerab

aDivision of Health, Design, and Science, University of Canberra, Canberra, ACT 2601, Australia, and bSan Ernesto, 6-Esc. 3, 28002 Madrid, Spain

10.2.2. Sealed sources and radiation-producing apparatus

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The types of source and apparatus covered in this section include: (1) sealed sources, such as those used for radiography, and for X-ray scattering experiments; (2) apparatus that produces ionizing radiations, such as X-ray generators and particle accelerators; (3) apparatus that produces ionizing radiation incidentally, such as electron microscopes, cathode-ray oscilloscopes, and high-voltage electronic rectifiers.

10.2.2.1. Enclosed installations

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Most modern equipment is produced in such a form as to meet the prevailing radiation-protection regulations of the country in which it is sold, and care must be taken that safety circuits provided by the manufacturer are not defeated by staff members undertaking setting-up procedures. Such safety devices might cause visual or audible signals to be given and turn off power to the irradiating device.

Many early X-ray generators, electron microscopes, etc. have by modern standards inadequate radiation-protection facilities. Where practicable, therefore, special enclosures should be fabricated to house the apparatus producing the ionizing radiation. These should be designed such that:

  • (i) no person should have access to the interior during irradiation;

  • (ii) access should be prevented during irradiation by the provision of fail-safe interlocks that turn off the irradiating source;

  • (iii) no person should be able to remain in an enclosure during irradiation;

  • (iv) a means of rapid exit should be available to an individual should by chance he (she) be within a enclosure when irradiation commences;

  • (v) the source can be turned off from within the enclosure;

  • (vi) during operation the dose equivalent at any accessible surface outside the enclosure shall not exceed 25 mSv (2.5 rem) per hour;

  • (vii) when not in use, sealed sources should be capable of being housed, by remote control, within suitable shielding inside the enclosure;

  • (viii) all interlocks should be fail-safe enabling isolation of the source in the event of the loss of electrical power.

10.2.2.2. Open installations

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An open installation because of operational requirements cannot have many of the safeguards suggested in Subsection 10.2.2.1[link]. It is essential that extreme caution be exerted by the operators of such installations. They should bear in mind the following facts:

  • (i) almost all radiation injuries in X-ray diffraction laboratories are to the fingers of the operators and occur when setting up monochromators close to the radiation source. Necrosis of the skin occurs within seconds under these circumstances.

  • (ii) The beams scattered from single crystals are highly directional and very intense. Finding and monitoring these beams is usually difficult, and normal radiation monitors tend to underestimate the dose.

10.2.2.3. Sealed sources

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Sealed sources ought to be manipulated only by remote means such as forceps and long tongs. Shielding should be close to the source to minimize the risk of scattered radiation reaching other workers.

Sealed sources should be registered by the RSO according to nature and activity. He (or she) is also responsible for their physical integrity and for regular examinations to detect corrosion or other damage.

Note that high-activity neutron sources can activate their immediate housings and give rise to additional radiation hazards.

10.2.2.4. X-ray diffraction and X-ray analysis apparatus

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X-ray-generating devices such as sealed tubes and rotating-anode generators produce intense beams of small cross section and are capable of giving severe radiation burns within a second or so of exposure. Great care is necessary when working close to the exit port of these devices.

Apertures in the housing enclosing the X-ray source should be covered by a shutter when the source is not being used. Interlocking devices should exist to prevent the emission of X-rays when:

  • (i) the shutter is open without the analysing components and the beam stops being in place;

  • (ii) the analysing device is not properly in its position in relation to the housing.

Housings, shutters, shielded enclosures, and beam stops should be constructed such that the dose equivalent at any accessible point 0.05 m from their surface does not exceed 25 mSv for all practical operating conditions of the source.

Warning lights and illuminated signs should be fitted, interlocked such that they are lit when a shutter is open.

10.2.2.5. Particle accelerators

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The codification of rules for the safe operation of high-energy particle accelerators is not simple because the various ionizing radiations produced by them require different protective procedures.

Particle accelerators ought to be operated in an enclosure from a remote control room in which the dose equivalent rate does not exceed 25 mSv h−1. A lower dose rate (2.5 mSv h−1) is required in adjacent areas used by non-radiation workers.

The probability of mixed radiations (e.g. X-rays and neutrons) co-existing makes servicing hazardous and all maintenance should be performed under the supervision of the RSO.








































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