International
Tables for
Crystallography
Volume H
Powder diffraction
Edited by C. J. Gilmore, J. A. Kaduk and H. Schenk
International Tables for Crystallography (2018). Vol. H, ch. 2.10, p. 212

Figure 2.10.35 

P. S. Whitfield,a* A. Huqb and J. A. Kadukc,d,e

aEnergy, Mining and Environment Portfolio, National Research Council Canada, 1200 Montreal Road, Ottawa ON K1A 0R6, Canada,bChemical and Engineering Materials Division, Spallation Neutron Source, P.O. Box 2008, MS 6475, Oak Ridge, TN 37831, USA,cDepartment of Chemistry, Illinois Institute of Technology, 3101 South Dearborn Street, Chicago, IL 60616, USA,dDepartment of Physics, North Central College, 131 South Loomis Street, Naperville, IL 60540, USA, and ePoly Crystallography Inc., 423 East Chicago Avenue, Naperville, IL 60540, USA
Correspondence e-mail:  pamela.whitfield@psi.ch
[Figure 2.10.35]
Figure 2.10.35

Data from powdered sucrose on a Bragg–Brentano instrument, with the peak intensities normalized to the first reflection. The thin sample was prepared by sieving onto a low-background silicon plate made slightly tacky using hairspray. The inset shows that there is a slight peak shift between the two data sets as well as the predicted decay in relative intensities with the thin sample with 2θ angle.