International
Tables for
Crystallography
Volume H
Powder diffraction
Edited by C. J. Gilmore, J. A. Kaduk and H. Schenk

International Tables for Crystallography (2018). Vol. H, ch. 2.1, pp. 44-45

Section 2.1.6.3.4. Combi-optics

A. Kerna*

aBruker AXS, Östliche Rheinbrückenstrasse 49, Karlsruhe 76187, Germany
Correspondence e-mail: arnt.kern@bruker-axs.de

2.1.6.3.4. Combi-optics

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The steadily growing trend towards multipurpose instrumentation has led to a multitude of X-ray optics combined in single modules to eliminate reassembling and realignment. Such `combi-optics' are usually motorized and allow a fully automatic, software-controlled switch between different beam paths to switch between different instrument geometries or to optimize beam conditioning (e.g. high flux versus high resolution).

A frequent requirement is the ability to switch between the divergent-beam Bragg–Brentano and parallel-beam Debye–Scherrer geometries, which can be achieved by two combi-optics as illustrated in Fig. 2.1.23[link]. In this example, the incident-beam combi-optics consist of a variable slit and a Göbel mirror. When operating as a variable slit (Fig. 2.1.23[link]a), the parallel-beam path is blocked by the variable slit. Turning the variable slit parallel to the divergent beam (Fig. 2.1.23[link]b) enables the parallel beam and blocks the divergent beam. The diffracted-beam combi-optics consist of a set of two parallel-plate collimators, which are separated by a small gap. When turning the two parallel-plate collimators into the beam direction, only those diffracted rays running parallel to the collimator plates will reach the detector (Fig. 2.1.23[link]b). When turning the collimators by approximately 90°, the gap between the two collimators acts as a variable slit enabling a divergent beam (Fig. 2.1.23[link]a).

[Figure 2.1.23]

Figure 2.1.23 | top | pdf |

Incident and diffracted beam combi-optics for switching between (a) the Bragg–Brentano geometry and (b) the parallel-beam geometry. S: X-ray source; D: detector.

Significantly more sophisticated combi-optics are used in X-ray diffractometers that are mostly used for thin-film analysis. In Fig. 2.1.24[link] an example for two different incident-beam and four different diffracted-beam paths is shown, providing the choice between eight different beam paths depending on the properties of the specimen and the application requirements. The incident beam path is characterized by a fixed-target X-ray source equipped with a Göbel mirror, attached on a motorized mount. By rotating this arrangement by about 5°, the beam travels either through a rotary absorber followed by a two-bounce channel-cut monochromator and a slit (upper beam path, high-resolution setting), or just through a single slit (lower beam path, high-flux setting). The diffracted beam path represents a double-detector setup, typically consisting of a point detector (D1) and a position-sensitive detector (D2). For the point detector three different beam paths can be chosen by means of a switchable slit, which either sends the beam through a three-bounce channel-cut analyser, or through the same two-parallel-plate-collimator arrangement already discussed in Fig. 2.1.23[link], either acting as a parallel-plate collimator or a variable slit. A fourth beam path without any diffracted-beam X-ray optics allows use of the position-sensitive detector.

[Figure 2.1.24]

Figure 2.1.24 | top | pdf |

Example of the use of highly sophisticated incident- and diffracted-beam combi-optics in combination with a rotatable X-ray source and a double detector arm. This setup enables two different incident-beam and four different diffracted-beam paths, and thus provides a choice between eight different beam paths, depending on the properties of the specimen and the requirements of the application. S: X-ray source, S′: X-ray source rotated by about 5°, D1, D2: detectors.








































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