International
Tables for
Crystallography
Volume H
Powder diffraction
Edited by C. J. Gilmore, J. A. Kaduk and H. Schenk

International Tables for Crystallography (2018). Vol. H, ch. 2.7, p. 168

Section 2.7.16. Final remarks

A. Katrusiaka*

aFaculty of Chemistry, Adam Mickiewicz University, Poznań, Poland
Correspondence e-mail: katran@amu.edu.pl

2.7.16. Final remarks

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During the last 100 years, and particularly during the last few decades, high-pressure diffractometric techniques have been developed covering a broad range of research in different fields of science. It is simply impossible to present all aspects of high-pressure methodology in one chapter. Many books, book chapters and scientific papers have been written on high-pressure research and therefore I have chosen to present a `flavour' of high-pressure crystallography, rather than concentrating on all its aspects. Readers interested in specific subjects can find the required information in a number of instructive books (Hazen & Finger, 1982[link]; Eremets, 1996[link]; Holzapfel, 1997[link]; Katrusiak & McMillan, 2004[link]; Boldyreva & Dera, 2010[link]; McMahon, 2012[link]) and in numerous articles in research journals. This chapter is only an introduction and gives some useful reference information for high-pressure crystallographers.

It should be stressed that the sample-preparation techniques for high-pressure studies are relatively demanding. Therefore, diffraction studies are often `adjusted' to the form of the sample obtained in the high-pressure device. In particular, powder diffraction, single-crystal and spectroscopic measurements can be conducted on some synchrotron beamlines (see e.g. Dera et al., 2013[link]). Many experimental techniques complementary to high-pressure crystallographic studies have not been mentioned here.

It can be concluded that, over the years, high-pressure research has become quite popular in materials science and at present all over the world there are hundreds or even thousands of scientists capable of performing high-pressure experiments. Their scientific output is significant, and can be used as a guide for those interested in specific types of high-pressure research.

References

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