International
Tables for
Crystallography
Volume H
Powder diffraction
Edited by C. J. Gilmore, J. A. Kaduk and H. Schenk

© International Union of Crystallography 2018
International Tables for Crystallography (2018). Vol. H, ch. 2.9, p. 193

Figure 2.9.7 

W. van Beeka* and P. Pattisona,b

aSwiss–Norwegian Beamlines at ESRF, CS 40220, 38043 Grenoble CEDEX 9, France, and bLaboratory for Quantum Magnetism, Institute of Physics, Ecole Polytechnique Federale de Lausanne, CH-1015 Lausanne, Switzerland
Correspondence e-mail:  wouter@esrf.fr
[Figure 2.9.7]
Figure 2.9.7

Sequence of XRD measurements between 21 and 27° 2θ. On heating at a rate of 2° min−1 at <1% RH, sequential dehydration was observed, with the anhydrate observed at the highest temperature. The vertical axis represents intensity. The `time' (scan number) axis represents temperature from 298 to 498 K in 2° min−1 increments. Adapted from Robertson & Bish (2010[link]).