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Small-angle neutron scattering
International Tables for Crystallography (2012). Vol. F, ch. 19.4, pp. 575-582 [ doi:10.1107/97809553602060000870 ]
... that exists between 1H and 2H (henceforth termed H and D), to which we will return below. In brief, the scatter ... by replacing some or all of the H atoms with D atoms. This control greatly extends the range of problems that ... length distribution. It is easy to show that equals , where M is the second moment of given by The average ...
Specific deuteration, combination with X-ray measurements
International Tables for Crystallography (2012). Vol. F, Section 19.4.6.4, p. 580 [ doi:10.1107/97809553602060000870 ]
... are examples that illustrate the approaches. References Bilgin, N., Ehrenberg, M., Ebel, C., Zaccai, G., Sayers, Z., Koch, M. H. J., Svergun, D. I., Barberato, C., Volkov, V., Nissen, P. & Nyborg, J. ( ...
[more results from section 19.4.6 in volume F]
Solvent conditions
International Tables for Crystallography (2012). Vol. F, Section 19.4.5.3, p. 580 [ doi:10.1107/97809553602060000870 ]
Solvent conditions 19.4.5.3. Solvent conditions Background arises from the incoherent scattering of hydrogen. Consequently, the use of high levels of D2O in the buffer improves the background, but may not be innocuous, since high levels of D2O have been seen to induce aggregation. In cases where complexes with labelled subunits are ...
[more results from section 19.4.5 in volume F]
The statistical labelling method
International Tables for Crystallography (2012). Vol. F, Section 19.4.4.3, p. 580 [ doi:10.1107/97809553602060000870 ]
... dimer in a larger complex. Random introduction of equimolar labelled (D) and unlabelled (H) subunits will result in a mixture of ... prepared with an equimolar mixture of all H and all D so that HH:DD = 1:1. The difference in scattering ...
[more results from section 19.4.4 in volume F]
Use of forward scattering to measure molecular weights
International Tables for Crystallography (2012). Vol. F, Section 19.4.3.7, p. 579 [ doi:10.1107/97809553602060000870 ]
Use of forward scattering to measure molecular weights 19.4.3.7. Use of forward scattering to measure molecular weights The value of the scattering function at zero scattering angle, which is obtained by extrapolation using a Guinier plot, is related to the molecular weight of the particle. In the neutron small-angle scattering ...
[more results from section 19.4.3 in volume F]
Fundamental relationships
International Tables for Crystallography (2012). Vol. F, Section 19.4.2, pp. 575-577 [ doi:10.1107/97809553602060000870 ]
... length distribution. It is easy to show that equals , where M is the second moment of given by The average atom ... Ann. Phys. (Leipzig), 46, 809-823. Debye, P. & Bueche, A. M. (1949). Scattering by an inhomogeneous solid. J. Appl. Phys. 20, 518-525. Debye, P. & Pirenne, M. H. (1938). Über die Fourieranalyse von interferometrischen Messungen ...
Introduction
International Tables for Crystallography (2012). Vol. F, Section 19.4.1, p. 575 [ doi:10.1107/97809553602060000870 ]
... that exists between 1H and 2H (henceforth termed H and D), to which we will return below. In brief, the scatter ... by replacing some or all of the H atoms with D atoms. This control greatly extends the range of problems that ...
International Tables for Crystallography (2012). Vol. F, ch. 19.4, pp. 575-582 [ doi:10.1107/97809553602060000870 ]
... that exists between 1H and 2H (henceforth termed H and D), to which we will return below. In brief, the scatter ... by replacing some or all of the H atoms with D atoms. This control greatly extends the range of problems that ... length distribution. It is easy to show that equals , where M is the second moment of given by The average ...
Specific deuteration, combination with X-ray measurements
International Tables for Crystallography (2012). Vol. F, Section 19.4.6.4, p. 580 [ doi:10.1107/97809553602060000870 ]
... are examples that illustrate the approaches. References Bilgin, N., Ehrenberg, M., Ebel, C., Zaccai, G., Sayers, Z., Koch, M. H. J., Svergun, D. I., Barberato, C., Volkov, V., Nissen, P. & Nyborg, J. ( ...
[more results from section 19.4.6 in volume F]
Solvent conditions
International Tables for Crystallography (2012). Vol. F, Section 19.4.5.3, p. 580 [ doi:10.1107/97809553602060000870 ]
Solvent conditions 19.4.5.3. Solvent conditions Background arises from the incoherent scattering of hydrogen. Consequently, the use of high levels of D2O in the buffer improves the background, but may not be innocuous, since high levels of D2O have been seen to induce aggregation. In cases where complexes with labelled subunits are ...
[more results from section 19.4.5 in volume F]
The statistical labelling method
International Tables for Crystallography (2012). Vol. F, Section 19.4.4.3, p. 580 [ doi:10.1107/97809553602060000870 ]
... dimer in a larger complex. Random introduction of equimolar labelled (D) and unlabelled (H) subunits will result in a mixture of ... prepared with an equimolar mixture of all H and all D so that HH:DD = 1:1. The difference in scattering ...
[more results from section 19.4.4 in volume F]
Use of forward scattering to measure molecular weights
International Tables for Crystallography (2012). Vol. F, Section 19.4.3.7, p. 579 [ doi:10.1107/97809553602060000870 ]
Use of forward scattering to measure molecular weights 19.4.3.7. Use of forward scattering to measure molecular weights The value of the scattering function at zero scattering angle, which is obtained by extrapolation using a Guinier plot, is related to the molecular weight of the particle. In the neutron small-angle scattering ...
[more results from section 19.4.3 in volume F]
Fundamental relationships
International Tables for Crystallography (2012). Vol. F, Section 19.4.2, pp. 575-577 [ doi:10.1107/97809553602060000870 ]
... length distribution. It is easy to show that equals , where M is the second moment of given by The average atom ... Ann. Phys. (Leipzig), 46, 809-823. Debye, P. & Bueche, A. M. (1949). Scattering by an inhomogeneous solid. J. Appl. Phys. 20, 518-525. Debye, P. & Pirenne, M. H. (1938). Über die Fourieranalyse von interferometrischen Messungen ...
Introduction
International Tables for Crystallography (2012). Vol. F, Section 19.4.1, p. 575 [ doi:10.1107/97809553602060000870 ]
... that exists between 1H and 2H (henceforth termed H and D), to which we will return below. In brief, the scatter ... by replacing some or all of the H atoms with D atoms. This control greatly extends the range of problems that ...
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