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The optics and alignment of the divergent-beam laboratory X-ray powder diffractometer and its calibration using NIST standard reference materials
Cline, J.P., Mendenhall, M.H., Black, D., Windover, D. and Henins, A.  International Tables for Crystallography (2018). Vol. H, ch. 3.1, pp. 224-251 [ doi:10.1107/97809553602060000946 ]
... rays striking the centre line of the PSD, outlined in black, are in accordance with Bragg-Brentano focusing. A monochromator can ... slits define divergence angle Acceptance angles [Delta]I and [Delta]D of the incident- and diffracted-beam Soller slits else to ... This is obtained by differentiating Bragg's law to obtain d[theta]/d[lambda]. The dominant term in the ...

Instrument calibration
Cline, J.P., Mendenhall, M.H., Black, D., Windover, D. and Henins, A.  International Tables for Crystallography (2018). Vol. H, Section 3.1.6, pp. 241-250 [ doi:10.1107/97809553602060000946 ]
... properly used, the method is capable of reporting the `true' d-spacing for profiles located in the 40 to 120░ 2 ... Applications of X-ray Diffraction, edited by F. H. Chung & D. K. Smith, pp. 903-917. New York: Marcel Dekker, Inc.GoogleScholar ... . J. Res. NIST, 120, 223-251.GoogleScholar Thompson, P., Cox, D. E. & Hastings, J. B. (1987). Rietveld refinement of ...

Data-analysis methods
Cline, J.P., Mendenhall, M.H., Black, D., Windover, D. and Henins, A.  International Tables for Crystallography (2018). Vol. H, Section 3.1.5, pp. 238-241 [ doi:10.1107/97809553602060000946 ]
... the observed profile maxima do not necessarily correspond to the d-spacing of the diffracting plane (hkl), except perhaps in a ... Laboratory, UK. http://www.ccp14.ac.uk/. GoogleScholar Finger, L. W., Cox, D. E. & Jephcoat, A. P. (1994). A correction for powder ... Cryst. 10, 66-68.GoogleScholar Hastings, J. B., Thomlinson, W. & Cox, D. E. (1984). Synchrotron X-ray powder diffraction. J. ...

SRMs, instrumentation and data-collection procedures
Cline, J.P., Mendenhall, M.H., Black, D., Windover, D. and Henins, A.  International Tables for Crystallography (2018). Vol. H, Section 3.1.4, pp. 235-238 [ doi:10.1107/97809553602060000946 ]
... of powder-diffraction equipment and measurements (NIST, 2015a ,b ,c ,d ). These SRMs can be divided into various categories based ... minimize off-axis stress on the 2[theta] rotation stage (Black et al., 2011 ). Thus, the goniometer assembly is exceedingly ... ray diffraction line-profile analysis. Powder Diffr. 10, 129-139.GoogleScholar Black, D. R., Windover, D., Henins, A., Filliben, J. & Cline, ...

Instrument alignment
Cline, J.P., Mendenhall, M.H., Black, D., Windover, D. and Henins, A.  International Tables for Crystallography (2018). Vol. H, Section 3.1.3, pp. 230-235 [ doi:10.1107/97809553602060000946 ]
Instrument alignment 3.1.3. Instrument alignment Modern instruments embody the drive towards interchangeable pre-aligned or self-aligning optics, which, in turn, has led to several approaches to obtaining proper alignment with minimum effort on the part of the user. We will not review these approaches, but instead we decribe here the ...

The instrument profile function
Cline, J.P., Mendenhall, M.H., Black, D., Windover, D. and Henins, A.  International Tables for Crystallography (2018). Vol. H, Section 3.1.2, pp. 224-230 [ doi:10.1107/97809553602060000946 ]
... rays striking the centre line of the PSD, outlined in black, are in accordance with Bragg-Brentano focusing. A monochromator can ... slits define divergence angle Acceptance angles [Delta]I and [Delta]D of the incident- and diffracted-beam Soller slits else to ... This is obtained by differentiating Bragg's law to obtain d[theta]/d[lambda]. The dominant term in the ...

Introduction
Cline, J.P., Mendenhall, M.H., Black, D., Windover, D. and Henins, A.  International Tables for Crystallography (2018). Vol. H, Section 3.1.1, p. 224 [ doi:10.1107/97809553602060000946 ]
Introduction 3.1.1. Introduction The laboratory X-ray powder diffractometer has several virtues that have made it a principal characterization device for providing critical data for a range of technical disciplines involving crystalline materials. The specimen is typically composed of small crystallites (5-30Ám), which is a form that is suitable ...

Conclusions
Cline, J.P., Mendenhall, M.H., Black, D., Windover, D. and Henins, A.  International Tables for Crystallography (2018). Vol. H, Section 3.1.7, p. 250 [ doi:10.1107/97809553602060000946 ]
... al., 2015 ). References Cline, J. P., Mendenhall, M. H., Black, D., Windover, D. & Henins, A. (2015). The optics and alignment of ...

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